Top Document: Sci.chem FAQ - Part 4 of 7 Previous Document: 16. Laboratory Procedures Next Document: 18. Sensory properties of chemicals See reader questions & answers on this topic! - Help others by sharing your knowledge 17.1 Where do I find laboratory-scale procedures for organics? The best introductory handbooks are practical textbooks, eg "Organic" Vogel and "EPOC" Vogel. They provide a diverse range of experiments that soon help develop synthetic skills. If you master the preparations in Vogel you are at the stage where you can start to obtain papers from organic chemistry journals and reproduce their syntheses. There are also several texts that discuss techniques for purifying laboratory chemicals, eg [1] The parameters of common specialist synthetic procedures usually are fully described in specialist texts that will only normally be available in chemistry department libraries ( eg Palladium Reagents in Organic Syntheses [2]). Most educational institutions will have a structured laboratory programme to develop skills. 17.2 Where do I find laboratory-scale procedures for inorganics? Most synthetic chemistry of inorganics appears to be devoted more to complex organometallics, superacids and superconductors than common inorganics, but it is worth considering that, of the top fifteen industrial chemicals produced, the only organic compounds are ethylene, propylene, ethylene dichloride and urea. There are specialist texts available that describe how to purify inorganic laboratory reagents, eg [1]. I expect some inorganic chemists to berate me for not knowing the standard inorganic synthesis textbooks. ;-) 17.3 Where do I find industrial chemical process details? The standard text for common processes remains Shreve, and I must admit that I enjoy reading the 1945 first edition to obtain a good overview of an industry. McKetta provides excellent process design details, along with comparisons of various processes. Kirk Othmer provides an excellent update on the various processes and chemicals used extensively today. Kirk Othmer remains the first port of call, but Ullmann is a close second. Both of these provide extensive references to more specific texts. Industry journals, eg Hydrocarbon Processing, offer annual reviews of the processes used in their industry. Patent literature has to be treated cautiously, as it is not always immediately obvious which patents detail actual viable processes. Chemical engineering texts, eg Perry, provide comprehensive detail of the equipment and operational parameters. User Contributions:Top Document: Sci.chem FAQ - Part 4 of 7 Previous Document: 16. Laboratory Procedures Next Document: 18. Sensory properties of chemicals Part1 - Part2 - Part3 - Part4 - Part5 - Part6 - Part7 - Single Page [ Usenet FAQs | Web FAQs | Documents | RFC Index ] Send corrections/additions to the FAQ Maintainer: B.Hamilton@irl.cri.nz
Last Update March 27 2014 @ 02:12 PM
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