Patent application number | Description | Published |
20080234446 | PROCESS FOR TRANSPORTING IN THE TANK OF A TANK TRUCK OR TANKER SHIP A LIQUID MONOMER PHASE WITHDRAWN FROM A STORAGE VESSEL - A process for transporting a liquid monomer phase which has been withdrawn from a storage vessel and comprises methacrylic monomers to an extent of ≧90% by weight, in a tank truck or in a tanker ship, in which the liquid monomer phase is subjected to a separating operation on the route from the storage vessel into the tank of a tank truck or of a tanker ship in order to separate polymer of the monomer present in dissolved form in the liquid monomer phase. | 09-25-2008 |
20080255374 | PROCESS FOR CHARGING A LONGITUDINAL SECTION OF A CATALYST TUBE - A process for charging a longitudinal section of a catalyst tube with a homogeneous fixed catalyst bed section whose active composition is at least one multielement oxide or comprises elemental silver on an oxidic support body and whose geometric shaped catalyst bodies and shaped inert bodies have a specific inhomogeneity of their longest dimensions. | 10-16-2008 |
20080260605 | PROCESS FOR PREPARING AT LEAST ONE ORGANIC TARGET COMPOUND BY HETEROGENEOUSLY CATALYZED GAS PHASE PARTIAL OXIDATION - A process for preparing an organic target compound by heterogeneously catalyzed gas phase partial oxidation of an organic precursor compound with molecular oxygen in two oxidation reactor lines operated in parallel and removal of the target compound from the mixture of the product gas streams in a workup line, wherein the catalysts charge of one of the oxidation lines comprises a portion of catalyst over which the heterogeneously catalyzed gas phase partial oxidation has already been carried out for longer than over the portions of catalyst of the catalyst charge of the other oxidation reactor line. | 10-23-2008 |
20080269521 | PROCESS FOR STARTING-UP A HETEROGENEOUSLY CATALYZED PARTIAL GAS PHASE OXIDATION OF ACROLEIN TO ACRYLIC ACID OR OF METHACROLEIN TO METHACRYLIC ACID - A process for starting-up a heterogeneously catalyzed partial gas phase oxidation of acrolein to acrylic acid or of methacrolein to methacrylic acid over a fixed catalyst bed disposed in a tube bundle reactor cooled by a heat exchange medium, wherein the temperature of the heat exchange medium is ≧290° C. and the temperature of that reactor plate surface which faces the reaction gas entry mixture and the temperature of the reaction gas entry mixture itself are ≦285° C. | 10-30-2008 |
20080269522 | PROCESS FOR OPERATING AN EXOTHERMIC HETEROGENEOUSLY CATALYZED PARTIAL GAS PHASE OXIDATION OF AN ORGANIC STARTING COMPOUND TO AN ORGANIC TARGET COMPOUND - A process for operating an exothermic heterogeneously catalyzed partial gas phase oxidation of an organic starting compound in a tube bundle reactor cooled with a fluid heat carrier, in which an increase in the loading of the fixed catalyst bed disposed in the reaction tubes with the organic starting compound is preceded by an increase in the inlet temperature of the fluid heat carrier into the space surrounding the reaction tubes. | 10-30-2008 |
20080300414 | PROCESS FOR RECHARGING THE REACTION TUBES OF A TUBE BUNDLE REACTOR WITH A NEW FIXED CATALYST BED - A process for recharging the reaction tubes of a tube bundle reactor with a new fixed catalyst bed, in which a heterogeneously catalyzed partial gas phase oxidation of an organic compound had been performed beforehand in a preceding fixed catalyst bed comprising Mo-comprising multielement oxide active compositions to form a steam-comprising product gas mixture, in which, before the recharge, solid deposit which had been deposited on the tube inner walls and comprises molybdenum oxide and/or molybdenum oxide hydrate is brushed away with the aid of a brush. | 12-04-2008 |
20080312477 | PROCESS FOR CHARGING A REACTOR WITH A FIXED CATALYST BED WHICH COMPRISES AT LEAST ANNULAR SHAPED CATALYST BODIES K - A process for charging a reactor with a fixed catalyst bed which comprises at least one annular shaped support catalyst body K, in which, before the charging, fragments formed in the preparation of the shaped catalyst bodies K are removed by screening. | 12-18-2008 |
20080319224 | METHOD FOR THE HETEROGENEOUSLY CATALYZED PARTIAL DIRECT OXIDATION OF N-PROPANE TO ACRYLIC ACID - A method for the heterogeneously catalyzed partial direct oxidation of propane to acrylic acid in the gas phase, in which the reaction gas inlet mixture comprises cyclopropane as an impurity and the acrylic acid, after it has been converted from the product gas mixture into the liquid phase, is operated from the other constituents of the liquid phase with the aid of a separation by crystallization. | 12-25-2008 |
20090018347 | PROCESS FOR PURIFYING REMOVAL OF ACRYLIC ACID, METHACRYLIC ACID, N-VINYLPYRROLIDONE OR P-XYLENE CRYSTALS FROM THEIR SUSPENSION IN MOTHER LIQUOR - A process for purifying removal of acrylic acid, methacrylic acid, N-vinylpyrrolidone or p-xylene crystals from their suspension in mother liquor by means of a wash column with forced transport, whose shell of the process chamber is a metal wall, the wash column additionally being enveloped by a thermal insulation material having a water vapor barrier and a specific heat flow of >0.1 W/m | 01-15-2009 |
20090076232 | PROCESS FOR OPERATING A CONTINUOUS REMOVAL OF A TARGET PRODUCT X IN THE FORM OF FINE CRYSTALS OF THE TARGET PRODUCT X - A process for operating a continuous removal of a target product X in the form of fine crystals of a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in the secondary chamber of an indirect heat exchanger to which liquid phase P flows continuously with simultaneous continuous flow through the primary chamber of the indirect heat exchanger with a coolant, and continuous withdrawal of a crystal suspension S having a degree of crystallization Y from the secondary chamber in two operating states I and II, wherein the coolant temperature is lower, the mass flow of liquid phase P is greater and the molar proportion of the constituents other than the target product X in the liquid phase P in operating state II is greater than in operating state I. | 03-19-2009 |
20090076286 | PROCESS FOR OPERATING A CONTINUOUS REMOVAL OF A TARGET PRODUCT X IN THE FORM OF FINE CRYSTALS - A process for continuously removing a target product X in the form of fine crystals from a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in an indirect heat transferee, in which the crystal suspension formed is conducted out of the heat transferer first into a mixed buffer tank and, from there, fed to an apparatus for separating the crystal suspension into crystals and liquid phase, and wherein external measures dissipade the oversaturation of the crystal suspension fed to the buffer vessel with target product X. | 03-19-2009 |
20090171117 | METHOD FOR PRODUCING A MULTI METAL OXIDE CATALYST, METHOD FOR PRODUCING UNSATURATED ALDEHYDES AND/OR CARBOXYLIC ACIDS AND BAND CALCINATION DEVICE - A catalyst suitable for the gas-phase oxidation of organic compounds to α,β-unsaturated aldehydes and/or carboxylic acids and having an active phase comprising a multimetal oxide material is prepared by a process in which a particulate catalyst precursor which contains oxides and/or compounds of the elements other than oxygen which constitute the multimetal oxide material, which compounds can be converted into oxides, is prepared and said catalyst precursor is converted by calcination into a catalytically active form, wherein a stream of the particulate catalyst precursor is passed at substantially constant speed through at least one calcination zone at constant temperature for calcination. | 07-02-2009 |
20090221780 | PROCESS FOR STORING A MONOMER PHASE WHICH IS LIQUID UNDER THE CONDITIONS OF STORAGE - A process for storing a monomer phase which is liquid under the conditions of storage and comprises methacrylic monomers to an extent of ≧95% by weight and has been obtained by condensation out of a gaseous phase or by melting a crystalline phase, in a storage vessel, in which polymer of the monomer present in dissolved form in the liquid monomer phase is removed therefrom on the route from its generation into the storage vessel, and also a process for withdrawing liquid monomer phase from the storage vessel in which polymer of the monomer present in dissolved form in the monomer phase is likewise removed. | 09-03-2009 |
20100010238 | PROCESS FOR PRODUCING A RINGLIKE OXIDIC SHAPED BODY - A process for producing a ringlike oxidic shaped body by mechanically compacting a pulverulent aggregate introduced into the fill chamber of a die, wherein the outer face of the resulting compact corresponds to that of a frustocone. | 01-14-2010 |
20100022734 | PROCESS FOR SEPARATING ACRYLIC ACID PRESENT AS A MAIN CONSTITUENT AND GLYOXAL PRESENT AS A BY-PRODUCT IN A PRODUCT GAS MIXTURE OF A PARTIAL HETEROGENEOUSLY CATALYZED GAS PHASE OXIDATION OF A C3 PRECURSOR COMPOUND OF ACRYLIC ACID - A process for separating acrylic acid present as a main product and glyoxal present as a by-product in a product gas mixture of a partial gas phase oxidation of a C | 01-28-2010 |
20100069659 | PROCESS FOR PRODUCING GEOMETRIC SHAPED CATALYST BODIES - A process for producing geometric shaped catalyst bodies K whose active material is a multielement oxide of stoichiometry | 03-18-2010 |
20100069660 | PROCESS FOR PRODUCING GEOMETRIC SHAPED CATALYST BODIES - A process for producing geometric shaped catalyst bodies K whose active material is a multielement oxide of stoichiometry | 03-18-2010 |
20100152475 | PROCESS FOR CONTINUOUSLY PRODUCING GEOMETRIC SHAPED CATALYST BODIES K - A process for producing geometric shaped catalyst bodies K whose active material is a multielement oxide which comprises the element Mo, the elements Bi and/or V and one or more of the elements Co, Ni, Fe, Cu and alkali metals, in which sources of the different elements are used to obtain a finely divided mixture which is coarsened to a powder by press agglomeration, the coarsened powder is used to form, by press agglomeration, shaped bodies V which are separated into undamaged shaped bodies V | 06-17-2010 |
20100152482 | PROCESS FOR REDISSOCIATING MICHAEL ADDUCTS WHICH ARE PRESENT IN A LIQUID F AND HAVE BEEN FORMED IN THE PREPARATION OF ACRYLIC ACID OR ESTERS THEREOF - A process for redissociating Michael adducts which are present in a liquid F with a proportion by weight of ≧10% by weight and have been formed in the preparation of acrylic acid or esters thereof in a redissociating apparatus which comprises a pump P, a separating column K with separating internals and a circulation heat exchanger UW, wherein, for the purpose of supplying the cleavage energy, the pump P sucks in bottoms liquid from the bottom space of the separating column K and, via the circulation heat exchanger UW, continually recycles it into the bottom space above the level of the bottoms liquid, and wherein the pump P is a radial circulation pump with an open impeller. | 06-17-2010 |
20100197489 | METHOD OF CHARGING CATALYST TUBES OF A BUNDLE OF CATALYST TUBES IN A STRUCTURED FASHION - A method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion, in which uniformly predispensed portions of formulations of shaped catalyst bodies are used for producing a section of charge. | 08-05-2010 |
20100206821 | PROCESS FOR PURIFYING REMOVAL OF A CHEMICAL TARGET COMPOUND FROM A SUSPENSION OF CRYSTALS THEREOF IN MOTHER LIQUOR - A process for purifying removal of a chemical target compound from a suspension of crystals thereof in mother liquor in a wash column with forced transport of the crystal bed from the top downward, in which crystals are removed from the lower end of the crystal bed with a rotating removal device and melted, and a portion of the crystal melt is conducted back toward the crystal bed as wash melt, the removal device being secured with a drive shaft conducted into the wash column from the bottom through an inlet having a seal, said drive shaft being driven about its longitudinal axis by a drive unit for rotation and being mounted so as to be rotatable about its longitudinal axis in more than one bearing, such that the mounting in one of the bearings absorbs the downward force acting on the drive shaft, the mounting in two or more bearings absorbs forces acting radially outward from the drive shaft, and the mounting in one bearing is additionally capable of absorbing an upward force acting on the drive shaft. | 08-19-2010 |
20100286461 | PROCESS FOR CONTINUOUS HETEROGENEOUSLY CATALYZED PARTIAL DEHYDROGENATION OF AT LEAST ONE HYDROCARBON TO BE DEHYDROGENATED - A process for continuous heterogeneously catalyzed partial dehydrogenation of at least one hydrocarbon to be dehydrogenated in a reactor which is manufactured from a steel with specific elemental composition on its side in contact with the reaction gas, and also partial oxidations of the dehydrogenated hydrocarbon and the reactor itself. | 11-11-2010 |
20110036704 | PROCESS FOR REMOVAL OF ACRYLIC ACID FROM THE PRODUCT GAS MIXTURE OF A HETEROGENEOUSLY CATALYZED PARTIAL GAS PHASE OXIDATION OF AT LEAST ONE C3 PRECURSOR COMPOUND - A process for removal of a crude acrylic acid from a product gas mixture which comprises glyoxal as a by-product from a heterogeneously catalyzed partial gas phase oxidation of at least one C | 02-17-2011 |
20110038763 | PROCESS FOR CONTINUOUS HETEROGENEOUSLY CATALYZED PARTIAL DEHYDROGENATION OF AT LEAST ONE HYDROCARBON TO BE DEHYDROGENATED - A process for continuous heterogeneously catalyzed partial dehydrogenation of at least one hydrocarbon to be dehydrogenated in a reactor which is manufactured from a composite material which consists, on its side in contact with the reaction chamber, of a steel B with specific elemental composition which, on its side facing away from the reaction chamber, either directly or via an intermediate layer of copper, or of nickel, or of copper and nickel, is plated onto a steel A with specific elemental composition, and also partial oxidations of the dehydrogenated hydrocarbon and the reactor itself. | 02-17-2011 |
20110065953 | PROCESS FOR THE LONG-TERM OPERATION OF A HETEROGENEOUSLY CATALYZED PARTIAL GAS PHASE OXIDATION OF AN ORGANIC STARTING COMPOUND - A process for the long-term operation of a heterogeneously catalyzed partial gas phase oxidation of an organic starting compound, in which the reaction gas input mixture is partially oxidized over a fixed catalyst bed which is accommodated in two successive temperature zones A, B whose temperature is changed with increasing operating time such that the initially lower temperature increases and the difference between the two temperatures decreases. | 03-17-2011 |
20130005925 | AQUEOUS SOLUTION COMPRISING ACRYLIC ACID AND THE CONJUGATE BASE THEREOF - An aqueous solution containing 10% by weight of acrylic acid and its conjugate base. The solution further contains, based on the amount of acrylic acid and its conjugate base: at least 50 ppm of propionic acid and its conjugate base; at least 200 ppm of formic acid and its conjugate base; at least 3000 ppm of acetic acid and it conjugate base; at most 10 ppm of benzoic acid and its conjugate base; at most 10 ppm of maleic anhydride, maleic acid, and their conjugate bases; at most 10 ppm of phthalic anhydride, phthalic acid, and their conjugate bases; at most 50 ppm of acrolein; at most 50 ppm of benzaldehyde; at most 50 ppm of 2-furaldehyde; and at least 20 mol % of at least one alkali metal cation. A process for preparing this solution and the use of this solution for preparation of a polymer by free-radical polymerization. | 01-03-2013 |
20130006009 | PROCESS FOR CONTINUOUSLY PRODUCING GEOMETRIC SHAPED CATALYST BODIES K - A process for producing geometric shaped catalyst bodies K whose active material is a multielement oxide which comprises the element Mo, the elements Bi and/or V and one or more of the elements Co, Ni, Fe, Cu and alkali metals, in which sources of the different elements are used to obtain a finely divided mixture which is coarsened to a powder by press agglomeration, the coarsened powder is used to form, by press agglomeration, shaped bodies V which are separated into undamaged shaped bodies V | 01-03-2013 |