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WEYLAND AS

WEYLAND AS Patent applications
Patent application numberTitlePublished
20120135489METHOD OF ALCOHOL PRODUCTION - The present invention relates to a process for producing alcohol from a cellulosic material, said process comprising: hydrolyzing said cellulosic material with an aqueous acid to produce a hydrolysate; extracting acid and water from said hydrolysate with a water-miscible organic extraction solvent to yield (a) a first aqueous acidic solution containing said extraction solvent and (b) a residue containing sugars; subjecting said residue to an oligosaccharide cleavage reaction to yield an aqueous solution of fermentable sugars; fermenting said fermentable sugars and distilling alcohol from the resulting fermented mixture; contacting said first aqueous acidic solution with a water-immiscible liquid lipophilic solvent to yield a second aqueous acid solution and a solvent mixture of said extraction solvent and said liquid solvent; separating said solvent mixture to yield extraction solvent for recycling; and separating from said second aqueous acid solution an aqueous acid for recycling.05-31-2012
20110312055METHOD OF PRODUCTION OF ALCOHOL - The invention provides a process for producing alcohol from a cellulosic material, said process comprising: hydrolyzing said cellulosic material with an aqueous acid to produce a hydrolysate; extracting acid and water from said hydrolysate with a water-miscible organic extraction solvent to yield (a) a first aqueous acidic solution containing said extraction solvent and (b) a residue containing sugars; subjecting said residue to an oligosaccharide cleavage reaction to yield an aqueous solution of fermentable sugars; fermenting said fermentable sugars and distilling alcohol from the resulting fermented mixture; contacting said first aqueous acidic solution with a pressurized fluid lipophilic solvent in non-gaseous form, which fluid solvent is substantially water-immiscible and is gaseous at ambient conditions, to yield a second aqueous acid solution and a solvent mixture of said extraction solvent and said fluid solvent; depressurizing said solvent mixture to release said extraction solvent for recycling; and, optionally, concentrating said second aqueous acid solution for recycling.12-22-2011
20110294181PROCESS FOR THE PRODUCTION OF ALCOHOL - The invention provides a process for producing alcohol from a cellulosic material, said process comprising the steps of: (i) hydrolyzing said cellulosic material with an aqueous acid to produce a hydrolysate; (ii) extracting acid and water from said hydrolysate with a water-miscible organic extraction solvent to yield (a) a first aqueous acidic solution containing said extraction solvent and (b) a residue containing sugars, (iii) subjecting said residue to an oligosaccharide cleavage reaction to yield an aqueous solution of fermentable sugars; (iv) fermenting said fermentable sugars and distilling alcohol from the resulting fermented mixture; (v) evaporating said extraction solvent from said first solution to yield (a) a second aqueous acid solution containing no more than 10% wt., preferably no more than 5% wt., of said extraction solvent and (b) gaseous extraction solvent; (vi) condensing said gaseous extraction solvent for recycling; and, optionally, (vii) concentrating said second aqueous acid solution for recycling; wherein said extraction solvent is liquid at the temperature and pressure of step (ii), has a boiling point of from 25 to 60° C. at a pressure in the range 1 to 8 bar, and is such that water-soluble oligosaccharides are precipitated from solution by its addition in step (ii).12-01-2011