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Tate & Lyle Technology Ltd.

Tate & Lyle Technology Ltd. Patent applications
Patent application numberTitlePublished
20120095199Based-Assisted formation of Tin-Sucrose Adducts - A method of forming a sucrose-6-ester includes in sequence the steps of: a) contacting sucrose with a organotinbased acylation promoter in a solvent in the presence of a base selected from amines and basic alkali metal salts; b) removing water to form a tin-sucrose adduct; and c) contacting the tin-sucrose adduct with an acylating agent to form the sucrose- 6-ester. The sucrose-6-ester may then be converted to sucralose.04-19-2012
20120077972Chlorination of sucrose-6-esters - A method for the chlorination of a sucrose-6-acylate to produce a 4,1′,6′-trichloro-4,1′,6′-trideoxy-galactosucrose-β-acylate wherein said method comprises: (i) reacting the sucrose-6-acylate with a chlorinating agent in a reaction vehicle comprising a tertiary amide in order to chlorinate the 4, V and 6′ positions of the sucrose-6-acylate; and (ii) quenching the product stream of (i) to produce a 4,1′,6′-trichloro-4,1′,6′-trideoxy-galactosucrose-6-acylate; wherein before said quenching, a portion of the tertiary amide is removed.03-29-2012