| 20080242827 | Method for producing omni-meta aromatic polysulfonamide fiber - The invention relates to a method of preparing omni-meta aromatic polysulfonamide fiber which comprises three steps of preparing spinning dope, wet spinning and post treating. The said step of preparing spinning dope comprises the following steps: (1) dissolving 3,3′-diaminodiphenyl sulphone in a polar organic solvent and cooling it to −20˜20° C.; (2) adding m-phthaloyl chloride of the same mole of the 3,3′-diaminodiphenyl sulphone to carry out a polymerization reaction; (3) then adding an inorganic base of the same mole of 3,3′-diaminodiphenyl sulphone to neutralize the hydrogen chloride produced during the polymerization reaction. The spinning dope thus prepared has a polymer solid content of 10%-20%. The fiber prepared according to the method in the present invention has a greatly improved crimpability, and evidently increased elongation at break comparing with the conventional aromatic polysulfonamide fiber, so that the spinnability of resultant yarn is improved. | 10-02-2008 |
