Beijing University of Chemical Technology Patent applications |
Patent application number | Title | Published |
20140154165 | METHOD FOR PREPARING GRAPHENE BY USING TWO-DIMENSIONAL CONFINED SPACE BETWEEN THE LAYERS OF INORGANIC LAYERED MATERIALS - The present invention relates to a method for preparing graphene using the two-dimensional confined space between the layers of inorganic layered materials. Such method comprises the following steps: mix a soluble salt of a divalent metal ion M | 06-05-2014 |
20130273294 | CARBON NANORING AND METHOD FOR PREPARING THE SAME - The invention relates to a carbon nanoring and a method for preparing the same. The carbon nanoring according to the present invention is composed of monolayered or multilayered coaxial carbon rings, wherein the carbon ring has a structure similar to that of a closed ring system formed by graphite sheet being rolled, and each of an axial dimension and a radial dimension of the carbon nanoring is nanoscale with the axial dimension being smaller than the radial dimension. The invention further provides a method for preparing the above carbon nanoring including calcinating in an inert atmosphere or a reducing atmosphere a layered double hydroxides obtained by intercalating a long-chain alkyl anion and a carbon source molecule, growing a carbon nanoring within a confined region between layers under the catalysis of the metal element in layers, and removing the metal and the metal oxide by dissolving in an acid to obtain the carbon nanoring. By using this method, the carbon nanoring can be effectively controlled in terms of the axial dimension, the radial dimension, and the number of layers of the carbon ring thereof. The carbon nanoring provided by the present invention has the nano-ring shaped structure and the excellent properties of carbon materials, as well as more edge carbons and dangling bonds, and thus it has broad application prospects in such field as nanodevices, energy storage and sensing. | 10-17-2013 |
20130183525 | Methods of Preparing Polyimide Fibers with Kidney-Shaped Cross-Sections - The present disclosure provides polyimide fibers with kidney-shaped cross-section and their preparation methods thereof, falling within the technical field of polyimide fiber. Polyimide fibers with kidney-shaped cross-sections are prepared by a continuous, integrated approach, starting from a polyamic acid solution prepared by reacting an aromatic dianhydride with an aromatic diamine. PAA nascent fibers with kidney-shaped cross-sections are obtained by adopting a spinneret having circular orifices under wet spinning process. The kidney-shaped cross-sections are obtained by varying the processing condition, including spinning speed, coagulation bath composition, coagulation temperature, and depth of coagulation bath. After washing and drying, polyamic acid nascent fibers are converted to polyimide fibers with kidney-shaped cross-sections under thermal curing. The integrated preparation methods are suitable for mass industrial production. | 07-18-2013 |
20130158174 | ADDITIVES AND METHODS FOR TERMINATING POLYMERIZATION AND/OR REDUCING VISCOSITY OF POLYMER SOLUTION - The present disclosure provides an additive and a method for terminating polymerization and/or reducing viscosity of polymer solution. The additive comprises a carboxylic acid, an alcohol, a salt chosen from alkali metal salts, alkaline earth metal salts, ammonium salts, and any combination thereof, and optionally, water. The method of the present disclosure comprises adding the additive according to present disclosure into a polymer solution and mixing the resulting mixture. The additive of the present disclosure can terminate living polymer chain ends efficiently and can destroy catalytic active centers and can substantially reduce the viscosity of a polymer solution. | 06-20-2013 |
20130143731 | SUPPORTED NOBLE METAL CATALYST AND PROCESS FOR PREPARING THE SAME IN SITU - A supported noble metal catalyst and a process for preparing the same in situ are provided. Hexamethylenetetramine, a soluble divalent metal salt solution, a Al | 06-06-2013 |
20130137846 | POLYIMIDE FIBER WITH HIGH STRENGTH AND HIGH MODULUS AND ITS PREPARATION METHOD - A high-strength high-modulus polyimide fiber and its preparation method pertain to the technical field of high-performance organic fiber. This fiber includes the polyimide (PI) fiber made from 3,3′,4,4′-biphenyl tetracarboxylic diandhydride (BPDA), p-phenylenediamine (pPDA) and 2-(4-aminophenyl)-1H-benzimidazol-5-amine (BIA), wherein the molar ratio between PPDA and BIA is 1:10˜3:1. During the synthesis, other diamine and diandhydride monomers may also be added. In the preparation process, the gradient temperature reaction method and one-step continuous preparation method are adopted, the synthesis and processing difficulty caused by the increase of the content of BIA is overcome, the problem of poor uniformity and stability of fiber is solved and PI fiber with high strength and high modulus is obtained. Its strength may reach 4.5 GPa and modulus may reach 201 GPa. Moreover, the sources of the raw materials are extensive, the spinning process is continuous, the cost is low, the efficiency is high and industrial production may be realized. | 05-30-2013 |
20130131357 | METHOD FOR PREPARING WHITE CARBON BLACK MODIFIED BY SILANE COUPLING AGENT - The invention relates to a method for preparing silica modified by a silane coupling agent. The method comprises the following steps: preparing a kind of coupling agent sol solution by mixing the solvent, water, catalyst and coupling agent; uniformly dispersing silica into the sol solution by means of ultrasonic dispersion or shear dispersion to achieve a turbid solution with uniform dispersion and ideal particle size; and then stirring the turbid solution at a constant speed to make the coupling agent sol reacting with silica to prepare highly hydrophobic silica modified by the coupling agent through controlling the temperature and reaction time. The coupling agent sol solution is obtained by a sol-gel process and silica is uniformly dispersed in the coupling agent sol solution through combined action of various dynamic means to ensure the sufficient reaction between silica and coupling agent, thus to obtain silica modified by the coupling agent. | 05-23-2013 |
20120322647 | METHOD FOR ENHANCING HETEROGENEOUS ASYMMETRIC SELECTIVITY AND CATALYTIC ACTIVITY - A method for enhancing heterogeneous asymmetric selectivity and catalytic activity belongs to the field of catalytic asymmetric organic synthesis technology, the preparation method of the invention are as follows: firstly preparing the chiral | 12-20-2012 |
20120282706 | PREPARATION OF AN OPTICAL PH SENSOR BASED ON FLUORESCEIN AND 1-HEPTANESULFONIC ACID SODIUM CO-INTERCALATED LAYERED DOUBLE HYDROXIDE - This invention relates to the field of preparation technology of optical pH sensor by co-intercalated fluorescein and 1-heptanesulfonic acid sodium into layered double hydroxide. The sensor is composed by conductive materials and the surface LDH films by co-interacted FLU and HES. The synthesis method is: first: synthesis of LDH colloid suspension, subsequently, the FLU and HES co-intercalated LDH colloid solution was prepared following the ion-exchange method, then the thin film of FLU-HES/LDH was spreaded on the surface of the conductive material by electrophoretic deposition, and the oriental pH sensor was synthesized. The advantages of the present invention is: first, the LDH matrix provides chromophore molecules with a confined and stable environment; the novel electrophoretic deposition strategy in this work provides a method for precise control of thickness (ranging from nanometers to micrometers), and the oriental pH sensor show good pH responsive. | 11-08-2012 |
20120240821 | UV-SHIELDING MATERIAL BASED ON MG-AL LAYERED DOUBLE HYDROXIDE AND ITS APPLICATION IN ANTI-AGEING ASPHALT - The present invention relates to a preparation method for a UV-shielding material based on Mg—Al Layered Double Hydroxide. The material with multi-layered overlay structure is made from Mg—Al double hydroxide layers and interlayer carbonate, its molecular composition is: Mg | 09-27-2012 |
20120228797 | Methods of Continuously Manufacturing Polymide Fibers - Methods for making high quality polyimide fibers suitable for continuous industrial production are described. Polyimide fibers are continuously prepared from a polyamic acid solution through sequentially spinning the polyamic acid solution by either a wet or a dry-wet process, coagulating, drying or drying after washing, thermally treating and stretching the resulting polyamic acid fibers to obtain polyimide fibers, and winding polyimide fibers as prepared into rolls. | 09-13-2012 |
20120168375 | METHOD FOR TREATING WASTE SALINE WATER PRODUCED IN PRODUCTION PROCESS OF DIPHENYLMETHANE DIISOCYANATE (MDI) - The invention relates to a method of circular use of waste brine produced in the manufacture process of MDI, comprising the following steps: (1) the waste brine produced in the manufacture process of MDI is subjected to a high-gravity extraction and then to a column extraction, wherein said waste brine contains aniline, diaminodiphenylmethane and polyamine; (2) the waste brine from step (1) is transmitted to a stripping tower for steam stripping; (3) the waste brine from the stripping tower of step (2) and a chemical oxidant are transmitted to an oxidation reactor to which air is blown for aeration; (4) the waste brine after the treatment of step (3) is transmitted to an absorption tower for absorption. The invention makes the salt water have TOC of less than 8 ppm and TN of less than 2.5 ppm and achieves regeneration of resources in the waste brine such as sodium chloride and water and the like for circular use. | 07-05-2012 |
20120088897 | EXTREME LOW FORMALDEHYDE EMISSION UF RESIN WITH A NOVEL STRUCTURE AND ITS PREPARATION - The present invention relates to an extreme low formaldehyde emission UF resin with a novel structure, and a process for its preparation. This UF resin is produced from formaldehyde, urea, a long chain multi-aldehyde prepolymer, and some modifiers. Its process follows three steps: weak caustic, weak acid and weak caustic. By using this prepolymer, the modified UF resin has stable alkyl ether structure, and the residual aldehyde groups on the UF polymer chain could accelerate cross-linking instead of dissociative formaldehyde. The UF resin made from this invention has extreme low dissociative formaldehyde and simple technology. The boards produced from this resin have good physical performance and water resistance. Moreover, the formaldehyde emission of the boards is extreme low, achieving Japan F⋆⋆⋆⋆ grade, the average emission value≦0.3 mg/L. | 04-12-2012 |
20120012793 | LEAD-FREE X-RAY SHIELDING RUBBER COMPOSITE - An overall lead-free X-ray shielding rubber compound material. The overall lead-free X-ray shielding rubber compound material uses rare earth mixture to replace lead, simultaneously adds metal tin and compounds thereof, metal tungsten and compounds thereof and bismuth and compounds thereof as shielding main materials and is further compounded with rubber to prepare the compound material which can realize the overall shielding and the complete lead-free property within the energy range of 40-170 kVp. When rare earth and bismuth materials are used, the way of combined use of two metal element inorganic compounds and unsaturated organic complexes is adopted, and the in-situ reaction and the compounding with a polymer matrix are carried out, thereby leading the shielding element disperse phase to form nano-micro-level dispersed particles. | 01-19-2012 |
20110268646 | PREPARATION METHOD OF CARBON NANOTUBE BY DECOMPOSING THE POLYMER WITH HYDROTALCITE AS A CATALYST - The present invention discloses a preparation method of carbon nanotube by decomposing the polymer with hydrotalcite as a catalyst, which belongs to the field of preparation technology of carbon nanotube (CNT). The technical solution of the present invention are as below: firstly, the hydrotalcite with the particle size at nanometer or sub-micron level is prepared, and then is added into the polymer. After the calcination process at high temperature and a treatment with acid, the nano-scale CNT can be obtained. The CNTs prepared by the method supplied in this invention not only have the advantages including high yield, uniform diameter, few structural defects, low impurity content, low cost and simple preparation process, which is suitable for large-scale industrial production, but also can solve the problem of recirculation of waste plastics and utilization of the resource. | 11-03-2011 |
20110237430 | PROCESS FOR PREPARING CATALYST COMPRISING PALLADIUM SUPPORTED ON CARRIER WITH HIGH DISPERSION - A process for preparing a catalyst comprising palladium supported on a carrier via a layered precursor, comprising the following steps: (1) synthesis of hydrotalcite layered precursor which comprises promoting metal element and aluminium on the surface of the carrier of Al | 09-29-2011 |
20110214979 | REACTIVE DISTILLATION APPARATUS FOR A MULTISTAGE COUNTER-CURRENT ROTATING BED AND ITS APPLICATION - The present invention discloses a reactive distillation apparatus for multistage counter-current rotating bed and its application, the apparatus comprises a closed shell, in the center of which a revolving shaft linking each shell section is set, the said shaft is provided with two or more rotors in series connection, a feeding inlet, a reflux inlet and an outlet of the gas phase are mounted on the top end face of the shell while a waste liquid outlet and an inlet of the gas phase are set on the bottom end face of the shell, the said shell consists of an upper section of the shell and a lower section of the shell along the axial direction, the said rotor consists of a rotating disc firmly connecting with the revolving shaft and a static disc mounted to the shell, a group of concentric dynamic filler rings but with different diameters are installed at intervals along the radial direction, wherein the wall of the dynamic filler rings is holed, and the ring clearance between the dynamic filler rings is configured with static rings fastened on the static disc; the filler filled in the said dynamic filler ring includes a catalytic filler and a wire gauze filler with the catalyst filler filled in the dynamic filler ring of the outer circle of the upper rotor and the inner circle of the lower rotor and the wire gauze filler filled in the rest of the dynamic filler rings, to make the whole rotor structure equivalent to the distillation section, reactive distillation section and stripping section; a feeding inlet is arranged on the top cover of the shell corresponding to the spray nozzle of raw material liquid; a rotating liquid distributor is arranged on the inner side of the innermost dynamic filler ring of the said lower rotor. The catalyst of the present invention not only plays the role of catalytic reaction, but also increases the interphase mass transfer area; the present invention improves the mass transfer efficiency and the separation efficiency of the reactive distillation process. | 09-08-2011 |
20110124766 | METHOD OF ULTRAVIOLET LIGHT ASSISTED SURFACE MODIFICATION AN PRODUCT HAVING A SURFACE FORMED BY THIS METHOD - The present invention relates to a UV irradiation assisted method of surface modification, which comprises: introducing a functional group L onto the surface of a polymer material P through the photochemical reaction of a photosensitive group X under UV irradiation, wherein the photosensitive group X comprises at least one xanthone unit. | 05-26-2011 |
20080220255 | CaCO3/SiO2 nH2O NANOCOMPOSITE PARTICLES AND SiO2 nH2O HOLLOW-STRUCTURES NANOMATERIALS AND SYNTHESIZING METHOD - The invention provides CaCO | 09-11-2008 |